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ABSTRACT Topological dislocations and stacking faults greatly affect the performance of functional crystalline materials1,2,3. Layer-stacking domain walls (DWs) in graphene alter its
electronic properties and give rise to fascinating new physics such as quantum valley Hall edge states4,5,6,7,8,9,10. Extensive efforts have been dedicated to the engineering of dislocations
to obtain materials with advanced properties. However, the manipulation of individual dislocations to precisely control the local structure and local properties of bulk material remains an
outstanding challenge. Here we report the manipulation of individual layer-stacking DWs in bi- and trilayer graphene by means of a local mechanical force exerted by an atomic force
microscope tip. We demonstrate experimentally the capability to move, erase and split individual DWs as well as annihilate or create closed-loop DWs. We further show that the DW motion is
highly anisotropic, offering a simple approach to create solitons with designed atomic structures. Most artificially created DW structures are found to be stable at room temperature. Access
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DOMINO-LIKE STACKING ORDER SWITCHING IN TWISTED MONOLAYER–MULTILAYER GRAPHENE Article 21 April 2022 UNCONVENTIONAL NON-LOCAL RELAXATION DYNAMICS IN A TWISTED TRILAYER GRAPHENE MOIRÉ
SUPERLATTICE Article Open access 08 December 2022 CONTROLLED ALIGNMENT OF SUPERMOIRÉ LATTICE IN DOUBLE-ALIGNED GRAPHENE HETEROSTRUCTURES Article Open access 12 July 2023 REFERENCES * Zou, X.
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Google Scholar Download references ACKNOWLEDGEMENTS We acknowledge helpful discussions with M. Asta, D. Chrzan, B. Yacobson, M. Poschmann and R. Zucker. We thank A. Zettl, Y. Zhang, T.
Wang and Y. Sheng for their help on sample preparation. The near-field infrared nanoscopy measurements and plasmon analysis was supported by the Director, Office of Science, Office of Basic
Energy Sciences, Materials Sciences and Engineering Division of the US Department of Energy under contract no. DE-AC02-05-CH11231 (Sub-wavelength Metamaterial Program) and National Key
Research and Development Program of China (grant number 2016YFA0302001). The bilayer graphene DW sample fabrication and characterization is supported by the Office of Naval Research (award
N00014-15-1-2651). L.J. acknowledges support from International Postdoctoral Exchange Fellowship Program 2016 (No.20160080). Z.S. acknowledges support from the Program for Professor of
Special Appointment (Eastern Scholar) at Shanghai Institutions of Higher Learning. AUTHOR INFORMATION Author notes * Lili Jiang and Sheng Wang contributed equally to this work. AUTHORS AND
AFFILIATIONS * Department of Physics, University of California at Berkeley, Berkeley, CA, USA Lili Jiang, Sheng Wang, Chenhao Jin, M. Iqbal Bakti Utama, Sihan Zhao, Yuen-Ron Shen & Feng
Wang * University of Chinese Academy of Sciences and Institute of Physics, Chinese Academy of Sciences, Beijing, China Lili Jiang & Hong-Jun Gao * Materials Science Division, Lawrence
Berkeley National Laboratory, Berkeley, CA, USA Sheng Wang, M. Iqbal Bakti Utama, Yuen-Ron Shen & Feng Wang * Key Laboratory of Artificial Structures and Quantum Control (Ministry of
Education), School of Physics and Astronomy, Shanghai Jiao Tong University, Shanghai, China Zhiwen Shi * Collaborative Innovation Center of Advanced Microstructures, Nanjing, China Zhiwen
Shi * Institute of Physics, Chinese Academy of Sciences, Beijing, China Guangyu Zhang * Kavli Energy NanoSciences Institute at the University of California, Berkeley and the Lawrence
Berkeley National Laboratory, Berkeley, CA, USA Feng Wang Authors * Lili Jiang View author publications You can also search for this author inPubMed Google Scholar * Sheng Wang View author
publications You can also search for this author inPubMed Google Scholar * Zhiwen Shi View author publications You can also search for this author inPubMed Google Scholar * Chenhao Jin View
author publications You can also search for this author inPubMed Google Scholar * M. Iqbal Bakti Utama View author publications You can also search for this author inPubMed Google Scholar *
Sihan Zhao View author publications You can also search for this author inPubMed Google Scholar * Yuen-Ron Shen View author publications You can also search for this author inPubMed Google
Scholar * Hong-Jun Gao View author publications You can also search for this author inPubMed Google Scholar * Guangyu Zhang View author publications You can also search for this author
inPubMed Google Scholar * Feng Wang View author publications You can also search for this author inPubMed Google Scholar CONTRIBUTIONS F.W. and Z.S. conceived the project. F.W., Y.-R.S. and
H.-J.G. supervised the project. G.Z. helped to design the study with Z.S. and F.W. L.J., Z.S. and C.J. performed the near-field infrared measurements and DW manipulation work. S.W. and L.J.
performed the SVM measurement. L.J. and S.Z. made the FET devices. M.I.B.U. carried out the SEM measurements. L.J., S.W., Z.S. and F.W. analysed the data. All authors discussed the results
and contributed to writing the manuscript. CORRESPONDING AUTHORS Correspondence to Zhiwen Shi or Feng Wang. ETHICS DECLARATIONS COMPETING INTERESTS The authors declare no competing financial
interests. ADDITIONAL INFORMATION PUBLISHER’S NOTE: Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations. SUPPLEMENTARY
INFORMATION SUPPLEMENTARY INFORMATION Supplementary Figures 1–10, Supplementary References. RIGHTS AND PERMISSIONS Reprints and permissions ABOUT THIS ARTICLE CITE THIS ARTICLE Jiang, L.,
Wang, S., Shi, Z. _et al._ Manipulation of domain-wall solitons in bi- and trilayer graphene. _Nature Nanotech_ 13, 204–208 (2018). https://doi.org/10.1038/s41565-017-0042-6 Download
citation * Received: 21 April 2017 * Accepted: 05 December 2017 * Published: 22 January 2018 * Issue Date: March 2018 * DOI: https://doi.org/10.1038/s41565-017-0042-6 SHARE THIS ARTICLE
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